Preparation and properties of epoxy-modified thermosetting phenolic fiber

Abstract: This article proposes the preparation and microwave thermal cured (MTC) epoxy-modified phenolic fibers for the first time. Epoxy-modified thermoplastic phenolic resin was first prepared in acidic condition using phenol, formaldehyde, and epichlorohydrin as the reactants, and then underwent additive reaction with formaldehyde to obtain epoxy-modified thermosetting phenolic resin, which was converted into nascent fibers through wet spinning. Finally, epoxy-modified phenolic fibers were obtained through different curing methods including solution cured, solution thermal cured, microwave cured, MTC, and was characterized by infrared spectroscopy, microscopic infrared imaging, nuclear magnetic resonance, thermogravimetric analysis, and scanning electron microscopy. The experiment results show that MTC epoxy-modified phenolic fibers have optimal mechanical property with ultimate elongation of 4% and breaking strength of 133 MPa.

Location
Deutsche Nationalbibliothek Frankfurt am Main
Extent
Online-Ressource
Language
Englisch

Bibliographic citation
Preparation and properties of epoxy-modified thermosetting phenolic fiber ; volume:23 ; number:1 ; year:2023 ; extent:11
e-Polymers ; 23, Heft 1 (2023) (gesamt 11)

Creator
Yin, YaoWen
Jiao, MingLi
Liu, AnFei
Wang, Hao
Liu, Yang
Liu, Ying
Yang, Kai
Zhu, GenXing

DOI
10.1515/epoly-2022-8085
URN
urn:nbn:de:101:1-2023031113040370493122
Rights
Open Access; Der Zugriff auf das Objekt ist unbeschränkt möglich.
Last update
14.08.2025, 10:47 AM CEST

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Associated

  • Yin, YaoWen
  • Jiao, MingLi
  • Liu, AnFei
  • Wang, Hao
  • Liu, Yang
  • Liu, Ying
  • Yang, Kai
  • Zhu, GenXing

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