Simple and convenient two step synthesis of 5-bromo-2,3-dimethoxy-6-methyl-1,4-benzoquinone
Abstract: 5-bromo-2,3-dimethoxy-6-methyl-1,4-benzoquinone 3, a key intermediate for preparing coenzyme Q compounds, was readily synthesized in two steps by a reaction sequence starting from the commercially available 3,4,5-trimethoxytoluene 1 via bromination and oxidation reactions. Persulfate salts were first employed as oxidants to synthesize 1,4-benzoquinone, the overall yield of title compound 3 was 65%.
- Location
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Deutsche Nationalbibliothek Frankfurt am Main
- Extent
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Online-Ressource
- Language
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Englisch
- Bibliographic citation
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Simple and convenient two step synthesis of 5-bromo-2,3-dimethoxy-6-methyl-1,4-benzoquinone ; volume:8 ; number:1 ; year:2019 ; pages:825-827 ; extent:3
Green processing & synthesis ; 8, Heft 1 (2019), 825-827 (gesamt 3)
- Creator
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Qiu, Yong-Fu
Lu, Bin
Yan, Yi-Yu
Zhou, Jin
Wang, Jin
- DOI
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10.1515/gps-2019-0052
- URN
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urn:nbn:de:101:1-2501120427532.047639544515
- Rights
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Open Access; Der Zugriff auf das Objekt ist unbeschränkt möglich.
- Last update
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15.08.2025, 7:29 AM CEST
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Associated
- Qiu, Yong-Fu
- Lu, Bin
- Yan, Yi-Yu
- Zhou, Jin
- Wang, Jin
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