Visible‐Light‐Mediated Amide Synthesis in Deep Eutectic Solvents

Abstract: In the present study, for the first time environmentally friendly deep eutectic solvents (DESs) are used as reaction media to perform an efficient, simple and straightforward photocatalytic amide synthesis at room temperature using thioacids and amines. This method features mild conditions, a broad substrate scope, high yields (≤99%) under ambient conditions with air and moisture tolerance. Moreover, the applied operationally mild reaction conditions tolerate the presence of several different functional group substituents on the amine counterpart. Finally, the developed approach allows the recycling of the reaction medium and catalyst for at least three consecutive cycles without a significant decrease in the reaction yield.

Object Details

• Location: Deutsche Nationalbibliothek Frankfurt am Main
• Extent: Online-Ressource
• Language: Englisch

References and Relationships

• Bibliographic citation: Visible‐Light‐Mediated Amide Synthesis in Deep Eutectic Solvents ; day:01 ; month:08 ; year:2023 ; extent:8 ; Advanced synthesis & catalysis ; (01.08.2023) (gesamt 8)

Contributors, Places and Time

• Creator: Procopio, Debora ; Marset, Xavier ; Guillena, Gabriela ; Di Gioia, Maria Luisa ; Ramón, Diego J.

Further information

• DOI: 10.1002/adsc.202300725
• URN: urn:nbn:de:101:1-2023080215032873308142
• Rights: Open Access; Der Zugriff auf das Objekt ist unbeschränkt möglich.
• Last update: 14.08.2025, 10:54 AM CEST