One‐Pot Multicomponent Synthesis ofBis (diamino‐1,3,5‐triazines) under Microwave Irradiation
Abstract: A new method for the synthesis of bis (1,3,5‐triazine‐2,4‐diamines) was developed using a one‐pot multicomponent approach. The synthesis was performed using the acid‐catalyzed reaction of cyanoguanidine with amines and aldehydes, followed by dehydrogenative aromatization of the dihydrotriazine intermediates upon heating with alkali. Two types of bis (1,3,5‐triazine‐2,4‐diamines) were prepared using either piperazine as the bifunctional amine or terephthaldehyde as the bifunctional aldehyde thus affording products with a piperazine or p‐phenylene link between two 1,3,5‐triazine rings. The microwave‐assisted method allows fast and convenient synthesis of diverse bis (1,3,5‐triazine‐2,4‐diamines).
- Location
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Deutsche Nationalbibliothek Frankfurt am Main
- Extent
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Online-Ressource
- Language
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Englisch
- Bibliographic citation
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One‐Pot Multicomponent Synthesis ofBis (diamino‐1,3,5‐triazines) under Microwave Irradiation ; volume:7 ; number:44 ; year:2022 ; extent:10
ChemistrySelect ; 7, Heft 44 (2022) (gesamt 10)
- Creator
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Bin Shahari, Muhammad Syafiq
Tiekink, Edward R. T.
Dolzhenko, Anton V.
- DOI
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10.1002/slct.202203038
- URN
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urn:nbn:de:101:1-2022112214084099665034
- Rights
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Open Access; Der Zugriff auf das Objekt ist unbeschränkt möglich.
- Last update
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15.08.2025, 7:20 AM CEST
Data provider
Deutsche Nationalbibliothek. If you have any questions about the object, please contact the data provider.
Associated
- Bin Shahari, Muhammad Syafiq
- Tiekink, Edward R. T.
- Dolzhenko, Anton V.