One‐Pot Multicomponent Synthesis ofBis (diamino‐1,3,5‐triazines) under Microwave Irradiation

Abstract: A new method for the synthesis of bis (1,3,5‐triazine‐2,4‐diamines) was developed using a one‐pot multicomponent approach. The synthesis was performed using the acid‐catalyzed reaction of cyanoguanidine with amines and aldehydes, followed by dehydrogenative aromatization of the dihydrotriazine intermediates upon heating with alkali. Two types of bis (1,3,5‐triazine‐2,4‐diamines) were prepared using either piperazine as the bifunctional amine or terephthaldehyde as the bifunctional aldehyde thus affording products with a piperazine or p‐phenylene link between two 1,3,5‐triazine rings. The microwave‐assisted method allows fast and convenient synthesis of diverse bis (1,3,5‐triazine‐2,4‐diamines).

Location
Deutsche Nationalbibliothek Frankfurt am Main
Extent
Online-Ressource
Language
Englisch

Bibliographic citation
One‐Pot Multicomponent Synthesis ofBis (diamino‐1,3,5‐triazines) under Microwave Irradiation ; volume:7 ; number:44 ; year:2022 ; extent:10
ChemistrySelect ; 7, Heft 44 (2022) (gesamt 10)

Creator
Bin Shahari, Muhammad Syafiq
Tiekink, Edward R. T.
Dolzhenko, Anton V.

DOI
10.1002/slct.202203038
URN
urn:nbn:de:101:1-2022112214084099665034
Rights
Open Access; Der Zugriff auf das Objekt ist unbeschränkt möglich.
Last update
15.08.2025, 7:20 AM CEST

Data provider

This object is provided by:
Deutsche Nationalbibliothek. If you have any questions about the object, please contact the data provider.

Associated

  • Bin Shahari, Muhammad Syafiq
  • Tiekink, Edward R. T.
  • Dolzhenko, Anton V.

Other Objects (12)